dehydrogenation of c terpinene in a ball mill

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Solvent-free dehydrogenation of γ-terpinene in a ball mill , The present article reports on the solvent-free dehydrogenation of γ-terpinene (1) in a planetary ball mill affording p-cymene (2) as the predominant reaction product.

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Reaction parameters for oxidative dehydrogenation of γ-terpinene 9 to p-cymene 10 were studied in great detail by Stolle et al (Scheme 64) [5] It was found that potassium permanganate is the most efficient oxidant in mechanochemical reaction Alumina was used as milling auxiliary in planetary ball mill Pulverisette, with ZrO.

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